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Hydrazine hydrate (1:1) → HCID 178480237、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 反応物 | 4-(2-Fluorobenzoyl)-1-methylpiperidine | HCID 13180317 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178480237 | HCID 178480237 | 23.7% |
反応手順
An autoclave was charged with 10.0 g of 4-(2-fluorobenzoyl)-1-methylpiperidine and 14 ml of hydrazine hydrate. The reaction was heated at 150° for 20 hrs, cooled, and poured into water. The resultant solid was collected. The solid was recrystallized twice from toluene to yield 2.4 g (23.7%) of product, mp 168°-170° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04670447 |
| 出典データセット | uspto-grants-1987_06 |
| ORD ID | ord-cdd33599bdaa477e8b872b2930c887a2 |
| 出典メモ | uspto-grants-1987_06 |