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Diethylamine → 2-Propenoic acid, 3-(chlorodimethylsilyl)-2-propen-1-yl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | Chlorodimethylsilane | HCID 66108 | — |
| 反応物 | Propargyl acrylate | HCID 82655 | — |
| 反応物 | Silanol | HCID 142154 | — |
| 反応物 | N,N-diethylaminoacryloxypropenyldimethylchlorosilane | HCID 86741630 | — |
| 生成物 | 2-Propenoic acid, 3-(chlorodimethylsilyl)-2-propen-1-yl ester | HCID 54158181 | — |
反応手順
Acryloxypropenyldimethylchlorosilane was prepared by a modification of Example 2 of U.S. Patent 3,746,734, to Berger et. al., using propargyl acrylate and dimethylchlorosilane as reactants. This product was then reacted with diethylamine. The resulting N,N-diethylaminoacryloxypropenyldimethylchlorosilane was then condensed with the 12000 MW and 28000 MW silanol terminated silicones utilized in Examples 1-16. The resulting acrylate terminated silicones were designated D and E, respectively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04675346 |
| 出典データセット | uspto-grants-1987_06 |
| ORD ID | ord-85e7b92189dd4fb189d70890859470ec |
| 出典メモ | uspto-grants-1987_06 |