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Bromotriphenylmethane → 4,4-Dimethyl-1-iodo-3-triphenylmethoxy-trans-1-octene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromotriphenylmethane | HCID 11692 | — |
| 反応物 | 4,4-Dimethyl-1-iodo-trans-1-octen-3-ol | HCID 20465723 | — |
| 生成物 | 4,4-Dimethyl-1-iodo-3-triphenylmethoxy-trans-1-octene | HCID 20465743 | — |
反応手順
Treatment of 11.2 g. (0.0396 mole) of 4,4-dimethyl-1-iodo-trans-1-octen-3-ol (Example 996) with 12.8 g. of triphenylmethyl bromide in 50 ml. of pyridine and purification on Florisil®, all as described in Example 728 gives the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04343949 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-1fa9a87d56c3413db2b1af374588a12a |
| 出典メモ | uspto-grants-1982_08 |