化工社化工社 化学情報印刷レポート · 研究参考用
Pivaloyl chloride → 2-[[2-(2,2-Dimethylpropanoyloxy)acetyl]-[2-(2,2-dimethylpropanoyloxy)ethyl]amino]ethyl 2,2-dimethylpropanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pivaloyl chloride | HCID 62493 | — |
| 反応物 | N,N-Bis(2-hydroxyethyl)glycolamide | HCID 87097 | — |
| 生成物 | 2-[[2-(2,2-Dimethylpropanoyloxy)acetyl]-[2-(2,2-dimethylpropanoyloxy)ethyl]amino]ethyl 2,2-dimethylpropanoate | HCID 326795 | — |
反応手順
This compound was prepared from 73 g (0.6 mole) of trimethylacetyl chloride and 32.6 g (0.2 mole) of N,N-bis(hydroxyethyl)hydroxyacetamide by the procedure of Example 1. Its structure was established by infrared and nuclear magnetic resonance spectroscopy. It was a white solid with m.p. 51.4° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04346043 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-049523fb07564b258267657ba1485247 |
| 出典メモ | uspto-grants-1982_08 |