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HRID 6776作成日:2026年10月24日

Bromine → 2-Bromophenacyl Bromide

https://huagongshe.com/ja/reaction/6776

反応式

関与物質

役割名称HCID仕込み量
反応物BromineHCID 24408—
反応物2'-BromoacetophenoneHCID 75060—
溶媒Acetic AcidHCID 176—
生成物2-Bromophenacyl BromideHCID 2737522—

反応手順

Bromine (40.3 g, 0.25 mol) was added dropwise to a solution of 2′-Bromoacetophenone (50.0 g, 0.25 mol) in acetic acid (50 ml) over 1.5 hours at 15–20° C. The solution was then allowed to warm to room temperature and concentrated under reduced pressure to yield a crude product that was used without further purification.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07084135B1
出典データセットuspto-grants-2006_08
ORD IDord-eba8a3d7c9cc40e19409ef56651f619b
出典メモuspto-grants-2006_08