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5-Amino-2-fluorobenzonitrile → HCID 178495899、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Amino-2-fluorobenzonitrile | HCID 2737673 | — |
| 反応物 | N-Hydroxy-4-[(2-methoxyethyl)amino]-1,2,5-oxadiazole-3-carboximidoyl chloride | HCID 136330165 | — |
| 生成物 | HCID 178495899 | HCID 178495899 | 100% |
反応手順
The desired compound was prepared according to the procedure of Example 13, step A, using N-hydroxy-4-[(2-methoxyethyl)amino]-1,2,5-oxadiazole-3-carboximidoyl chloride [made according to Example 1, steps A through E] and 5-amino-2-fluorobenzonitrile [Aldrich, product #639877] as the starting materials in 100% yield. LCMS for C13H14FN6O3 (M+H)+: m/z=321.0.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822511B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-89e62062841d41d2a7281f88b9107064 |
| 出典メモ | uspto-grants-2014_09 |