化工社化工社 化学情報印刷レポート · 研究参考用
Malonic acid, disodium salt → Zinc Malonate Dihydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Malonic acid, disodium salt | HCID 8865 | — |
| 反応物 | Malonate Ion | HCID 9084 | — |
| 反応物 | Zincchloride | HCID 3007855 | — |
| 反応物 | Zinc L-glutamate Dihydrate | HCID 22825209 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Zinc Malonate Dihydrate | HCID 86616729 | — |
反応手順
Basically the reaction conditions found for preparation of zinc L-glutamate (Example 13) was employed. A suspension of sodium malonate (white coloured) is prepared by adding 100 mL of millipore water to 16.605 g (0.1 moles) of solid sodium malonate dibasic monohydrate (SIGMA M1875-100G, MW 166.05, CAS 26522-85-0) in a 250 mL beaker. To this suspension was added 13.628 g (0.1 moles) of solid zinc chloride (FLUKA, 96469, MW 136.3, CAS 7646-85-7). Subsequent manufacturing steps were as described in Example 13.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07589235B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-61926276b95f4951b769df7926e9ab35 |
| 出典メモ | uspto-grants-2009_09 |