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Cyclohexyl isocyanate → HCID 67354653、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexyl isocyanate | HCID 18502 | — |
| 反応物 | Potassium Bromide | HCID 253877 | — |
| 反応物 | Ethyl 3-(4-aminophenyl)isoxazole-5-carboxylate | HCID 53407704 | — |
| 反応物 | 3-[4-(3-Phenyl-ureido)-phenyl]-isoxazole-5-carboxylic acid ethyl ester | HCID 67352240 | — |
| 生成物 | HCID 67354653 | HCID 67354653 | 75% |
反応手順
The title compound was prepared from 3-(4-amino-phenyl)-isoxazol-5-carboxylic acid ethyl ester and cyclohexyl isocyanate by same procedure as set forth for the preparation of 3-[4-(3-phenyl-ureido)-phenyl]-isoxazole-5-carboxylic acid ethyl ester and was obtained in 75% yield. Mass (ES+), 358 (M++1); IR (KBr): 3304, 2928, 2852, 1731, 1634, 1570 (br); 1H NMR (DMSO-d6) δ: 1.33 (t, 3H), 1.14-1.81 (4×m, 10H), 3.45 (br, 1H), 4.37 (q, 2H), 6.18 (d, 1H), 7.50 (d, 2H), 7.60 (s, 1H), 7.79 (s, 1H), 7.8.1 (d, 2H), 8.59 (s, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08835428B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-53f4d7ff59f245f59e1bfcfa30d2f0b4 |
| 出典メモ | uspto-grants-2014_09 |