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2-Amino-4,5,6,7-tetrahydrobenzothiazole → 3-(2-methoxy-ethyl)-4,5,6,7-tetrahydro-3H-benzothiazol-2-ylideneamine hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4,5,6,7-tetrahydrobenzothiazole | HCID 18046 | — |
| 反応物 | 2-Bromoethyl methyl ether | HCID 80972 | — |
| 生成物 | 3-(2-methoxy-ethyl)-4,5,6,7-tetrahydro-3H-benzothiazol-2-ylideneamine hydrobromide | HCID 66859028 | — |
反応手順
A mixture of 4,5,6,7-tetrahydro-benzothiazol-2-ylamine (300 mg, 1.94 mmol) and 2-bromoethyl methyl ether (600 μL, 6.40 mmol) was processed according to the method of Example 12A to provide the title compound as crude product: MS (LC/MS) m/z 213 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841334B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-8847ec3281d5466a99cd84ae68050294 |
| 出典メモ | uspto-grants-2014_09 |