(Pyridin-4-yl)boronic acid → 4-(3,4'-Bipyridin-5-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

HRID 80438

反応式

HRID 80438 の反応式
Br[C:2]1[CH:3]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:5]=[N:6][CH:7]=1.[N:19]1[CH:24]=[CH:23][C:22](B(O)O)=[CH:21][CH:20]=1>>[N:6]1[CH:5]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:3]=[C:2]([C:22]2[CH:23]=[CH:24][N:19]=[CH:20][CH:21]=2)[CH:7]=1

参加物

3

反応物 2

HCID 2734379(Pyridin-4-yl)boronic acidHCID 866492494-(5-Bromopyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

生成物 1

HCID 866492564-(3,4'-Bipyridin-5-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

実験手順

The title compound was prepared from the product of Example 65A and 4-pyridinylboronic acid according to General Method B: LC-MS Method B (ESI+) m/z 307.0 (M+H)+, retention time 1.54 minutes.

出典と根拠

ORDレコード
ord-1f6c4fd4267d417c902c6d1379502707
出典データセット
uspto-grants-2014_09
特許番号
US08846661B2

関連ノート

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