化工社化工社 化学情報印刷レポート · 研究参考用
Piperonal → 6-Benzo[1,3]dioxol-5-yl-3-(2-chloro-phenyl)-5-methyl-5H-isoxazolo[4,5-c]pyridin-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperonal | HCID 8438 | — |
| 反応物 | 3-(2-chlorophenyl)-N,5-dimethyl-1,2-oxazole-4-carboxamide | HCID 798829 | — |
| 生成物 | 6-Benzo[1,3]dioxol-5-yl-3-(2-chloro-phenyl)-5-methyl-5H-isoxazolo[4,5-c]pyridin-4-one | HCID 22015573 | — |
反応手順
This compound is obtained using 3-(2-chloro-phenyl)-5-methyl-isoxazole-4-carboxylic acid methylamide and benzo[1,3]dioxole-5-carbaldehyde in 35% as a beige solid. Mass spectrum: m/z (M+H)+: 380.9, 382.9
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087756B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-99c9a33baecf43dd9a0f32dfc95cd8a1 |
| 出典メモ | uspto-grants-2006_08 |