化工社化工社 化学情報印刷レポート · 研究参考用
Phenol → (+)-4-(2-Methyldecanoyl) phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | Decanoic acid, 2-methyl- | HCID 91167 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | (+)-4-(2-Methyldecanoyl) phenol | HCID 53900693 | 40% |
反応手順
Then, the same procedure as in Example 1 was repeated except that the above (+)-2-methyl decanoic acid was used instead of (+)-2-methyl butanoic acid to convert this compound into an acid chloride, which was reacted with phenol through aluminum chloride in methylene chloride to obtain (+)-4-(2-methyldecanoyl) phenol having the aforementioned physical and chemical properties at a yield of 40%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05137653 |
| 出典データセット | uspto-grants-1992_08 |
| ORD ID | ord-7f0319ed762c4c32be7fbb428e598d7f |
| 出典メモ | uspto-grants-1992_08 |