化工社化工社 化学情報印刷レポート · 研究参考用
Water → N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | O-Xylene | HCID 7237 | — |
| 反応物 | Hexan-3-amine | HCID 86062 | — |
| 反応物 | 4-Allyl-3-methyl-2,6-dinitrochlorobenzene | HCID 20563841 | — |
| 生成物 | N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline | HCID 54001796 | — |
反応手順
One equivalent of 4-allyl-3-methyl-2,6-dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04297127 |
| 出典データセット | uspto-grants-1981_10 |
| ORD ID | ord-930fb5109d234756b6b766f79009173a |
| 出典メモ | uspto-grants-1981_10 |