化工社化工社 化学情報印刷レポート · 研究参考用
Phthalic Anhydride → N,N-Dibutylformamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | Phthaloyl chloride | HCID 6955 | — |
| 反応物 | Dibutylcarbamoyl chloride | HCID 83371 | — |
| 生成物 | N,N-Dibutylformamide | HCID 12975 | — |
反応手順
The crude product remains as a dark oil. According to HPLC analysis, it contains 83.8% by weight of phthaloyl chloride, 2.4% by weight of phthalic anhydride, and, according to GC analysis, 0.9 area % of N,N-dibutylcarbamoyl chloride. Based on the product, this corresponds to a crude yield of 97.8% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07154003B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-c40172eda5a949b1acf88fddb69d4519 |
| 出典メモ | uspto-grants-2006_12 |