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1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone → 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone | HCID 301557 | — |
| 反応物 | Sodium hypobromite | HCID 23673712 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid | HCID 2759552 | — |
反応手順
18 g of 4-acetyl-4'-methoxybiphenyl was dissolved in 285 ml of dioxane and oxidized with a dilute sodium hypobromite. The product was recrystallized in a mixture of ethanol and acetic acid to obtain 4'-methoxybiphenyl-4-carboxylic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04775223 |
| 出典データセット | uspto-grants-1988_10 |
| ORD ID | ord-69c6ca8319c74053be2bb8f6a32fc4fd |
| 出典メモ | uspto-grants-1988_10 |