化工社化工社 化学情報印刷レポート · 研究参考用
Benzaldehyde → Methanaminium, N-methyl-N-(phenylmethylene)-, chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 生成物 | Methanaminium, N-methyl-N-(phenylmethylene)-, chloride | HCID 11073839 | — |
反応手順
The reaction of 32.0 ml (0.213 mol) dimethylamine solution and 8.0 ml (0.079 mol) benzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 4.7 ml (0.079 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 9.5 g (corresponding to 70.7% of the yield calculated by theory) of benzylidene-dimethyl-ammonium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-a8a93c2e2b784f2fbed88552562dcb80 |
| 出典メモ | uspto-grants-2006_08 |