化工社化工社 化学情報印刷レポート · 研究参考用
Jasmonic Acid → Cyclopentaneacetic acid, 3-oxo-2-pentyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Jasmonic Acid | HCID 5281166 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Cyclopentaneacetic acid, 3-oxo-2-pentyl- | HCID 107126 | 100% |
反応手順
A mixture of 2.5 g (11.9 mmol) jasmonic acid (i.e. 2-(3-oxo-2-(2-pentenyl)cyclopentyl)acetic acid) and Pd/C (0.5 g) in THF (50 mL) was hydrogenated at room temperature for 4 h. The reaction mixture was filtered and the filtrate was concentrated to give 2-(3-oxo-2-(pentanyl)cyclopentyl)acetic acid (2.5 g, 100%) as yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09284274B2 |
| 出典データセット | uspto-grants-2016_03 |
| ORD ID | ord-77e18ef9347b4f978198555a7752cca6 |
| 出典メモ | uspto-grants-2016_03 |