化工社化工社 化学情報印刷レポート · 研究参考用
Chlorosulfonic acid → Ethyl 2-(4-(chlorosulfonyl)-2-ethylphenoxy)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorosulfonic acid | HCID 24638 | — |
| 反応物 | Ethyl (2-ethylphenoxy)acetate | HCID 21986411 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Ethyl 2-(4-(chlorosulfonyl)-2-ethylphenoxy)acetate | HCID 21986343 | — |
反応手順
A solution of crude ethyl(2-ethylphenoxy)acetate (intermediate 107) in chloroform (6 ml) was stirred with chlorosulfonic acid (1.33 ml) at ambient temperature for 4 hours. The reaction mixture was quenched by the addition of ice and the organic mixture separated by using a hydrophobic frit. The title compound was isolated by evaporation of this filtrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091237B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-1f39594965174048aec2d27ed501f246 |
| 出典メモ | uspto-grants-2006_08 |