関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Carbamic acid, N-methyl-, ethyl ester | HCID 7752 | — |
| 反応物 | 2-Butylphenol | HCID 18515 | — |
| 反応物 | Phosphorus tribromide | HCID 24614 | — |
| 生成物 | Butylphenyl n-methylcarbamate | HCID 22930593 | — |
反応手順
To a solution of 2-sec butylphenol (1.5 g, 0.01 mole) and ethyl N-methylcarbamate (1.03 g, 0.01 mole) was added phosphorus tribromide (2.7 g, 0.01 mole) and the contents were heated at 140° C. for 15 hours. The reaction mixture was worked up as described earlier to give 2-sec butylphenyl N-methylcarbamate, identified by spectral data.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05066819 |
|---|
| 出典データセット | uspto-grants-1991_11 |
|---|
| ORD ID | ord-946850588377445e9d0cc6de15bab121 |
|---|
| 出典メモ | uspto-grants-1991_11 |
|---|
