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2-Butylphenol → Butylphenyl n-methylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Butylphenol | HCID 18515 | — |
| 反応物 | Phosphorus tribromide | HCID 24614 | — |
| 反応物 | Methyl methylcarbamate | HCID 81151 | — |
| 溶媒 | 1,1-Dichloroethane | HCID 6365 | — |
| 生成物 | Butylphenyl n-methylcarbamate | HCID 22930593 | — |
反応手順
To a mixture of methyl N-methylcarbamate (0.89 g, 0.01 mole) and 2-sec butylphenol (1.5 g, 0.01 mole) in dichloroethane (10 ml), a solution of phosphorus tribromide (2.7 g, 0.01 mole) in dichloro-ethane (6 ml) was added and the mixture was refluxed for eight hours. It was then worked up and purified as described earlier to give 2-sec butylphenyl N-methylcarbamate of the formula (III).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05066819 |
| 出典データセット | uspto-grants-1991_11 |
| ORD ID | ord-09819cf810f24f4d84bbbf6a19b0dbed |
| 出典メモ | uspto-grants-1991_11 |