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Hydrochloric Acid → N-(3-pyrrolidyl)phthalimide hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-(1-benzylpyrrolidin-3-yl)phthalimide | HCID 6711061 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-(3-pyrrolidyl)phthalimide hydrochloride | HCID 22926344 | — |
反応手順
12.70 g of N-(1-benzylpyrrolidin-3-yl)phthalimide was dissolved in 100 ml of ethanol and then subjected to hydrogenating decomposition with addition of 1.0 g of 10% palladium-carbon and 5.2 ml of concentrated hydrochloric acid at 60° C. under 1 atm. After 12 hours, the catalyst was filtered out and the solvent was distilled off to obtain 11.03 g of N-(3-pyrrolidyl)phthalimide hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05607953 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-98f4c34f8a8948d9a5ee44965d3d076e |
| 出典メモ | uspto-grants-1997_03 |