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5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole → 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 54086563 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 19970945 | — |
反応手順
Obtained from the title compound of Example 42 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.50 (SS 4). C,73.39; H,8.77; N,9.06. C18H26N2O; 0.125 CH2Cl2 requires C,73.28; H,8.91; N,9.43%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05607960 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-631587a7f2de4c9a86ff6b175d215833 |
| 出典メモ | uspto-grants-1997_03 |