化工社化工社 化学情報印刷レポート · 研究参考用
HCID 14075472、化合物 → N,N-Diethyl-3-pyrrolidinemethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 14075472 | HCID 14075472 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N,N-Diethyl-3-pyrrolidinemethanamine | HCID 14075474 | 101.7% |
反応手順
A mixture of 25.4 g (0.10 mole) of N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine, 200 ml of methyl alcohol, 2 g of palladium on carbon and hydrogen were shaken at a pressure of 51.5 psi. After 20.3 hours, the catalyst was filtered and the filtrate concentrated under reduced pressure. The residue was bulb to bulb distilled giving 15.9 g of N,N-diethyl-3-pyrrolidinemethanamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04665079 |
| 出典データセット | uspto-grants-1987_05 |
| ORD ID | ord-e7febe3b43c34959b96b8427691a395a |
| 出典メモ | uspto-grants-1987_05 |