Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalic Acid → N-[3-(2-benzo[b]thiophen-5-ylethoxy)propyl]-N,N-diethylamine oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalic Acid | HCID 971 | — |
| 반응물 | N-[3-(2-benzo[b]thiophen-5-ylethoxy)propyl]-N,N-diethylamine | HCID 22666289 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | N-[3-(2-benzo[b]thiophen-5-ylethoxy)propyl]-N,N-diethylamine oxalate | HCID 22666288 | 78.1% |
반응 단계
In 2 mL of ethyl acetate is dissolved 0.46 g of N-[3-(2-benzo[b]thiophen-5-ylethoxy)propyl]-N,N-diethylamine, to which is added 2.5 mL of a solution of 0.15 g of oxalic acid in ethyl acetate. The resulting mixture is stirred at ambient temperature for 2 hours. The deposited crystal is collected by filtration, washed with ethyl acetate and dried to obtain 0.47 g of N-[3-(2-benzo[b]thiophen-5-ylethoxy)propyl]-N,N-diethylamine oxalate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06797726B1 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-1f0ea39af0b748bab5f24a13e5e63a32 |
| 출처 메모 | uspto-grants-2004_09 |