Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 2-Bromo-1-oxoindan-5-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 1-oxo-2,3-dihydro-1H-indene-5-carbonitrile | HCID 312896 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Bromo-1-oxoindan-5-carbonitrile | HCID 18407238 | — |
반응 단계
1-Oxoindane-5-carbonitrile is brominated with bromine in glacial acetic acid with addition of a catalytic amount of 48% strength HBr solution in water and affords 2-bromo-1-oxoindane-5-carbonitrile with a melting point of 115-118° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06476059B1 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-6e54ad14693d46c5a0dc92736c8e474b |
| 출처 메모 | uspto-grants-2002_11 |