Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl isoeugenol → 1,2-Dimethoxy-4-propylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl isoeugenol | HCID 7128 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1,2-Dimethoxy-4-propylbenzene | HCID 123233 | 97.2% |
반응 단계
An atmospheric pressure hydrogenation equipment was charged with 17.8 g (0.10 M) of 1,2-dimethoxy-4-propenylbenzene, 0.9 g of palladium charcoal and 350 ml of methanol and introduced with hydrogen. The reaction was continued until the absorption of hydrogen was terminated. Palladium charcoal was filtered off from the reaction mixture. The filtrate was distilled off methanol and vacuum distilled to obtain 17.5 g (0.097 M) of 4-propylveratrole as colorless transparent liquid having a boiling point of 106°-108° C./4 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05102906 |
| 출처 데이터셋 | uspto-grants-1992_04 |
| ORD ID | ord-002a110d04e34e528766e20cdf8af164 |
| 출처 메모 | uspto-grants-1992_04 |