Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloride methanol → HCID 178418896, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloride methanol | HCID 21893726 | — |
| 반응물 | HCID 178418932 | HCID 178418932 | — |
| 생성물 | HCID 178418896 | HCID 178418896 | — |
반응 단계
According to the method of Example 1, Step C, deprotection was performed (room temperature, 2 hours) by using Intermediate 121 (49.4 mg) and 10% hydrogen chloride/methanol solution (2 ml). The solvent was evaporated under reduced pressure, and the residue was added with methanol (0.5 ml) and diethyl ether (1.5 ml). The deposited precipitates were collected by filtration and washed with diethyl ether to obtain the title compound (44.3 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094789B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-4e85aeddbc554fecbb78e2baa0b93744 |
| 출처 메모 | uspto-grants-2006_08 |