Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl bromoacetate → Methyl (2-formyl-4-methoxyphenoxy)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 반응물 | 2-Hydroxy-5-methoxybenzaldehyde | HCID 95695 | — |
| 생성물 | Methyl (2-formyl-4-methoxyphenoxy)acetate | HCID 43212883 | 86% |
반응 단계
In the same manner as in Reference Example 1, 5-methoxysalicylaldehyde was reacted with methyl bromoacetate to yield methyl 2-formyl-4-methoxyphenoxyacetate (yield 86%), which was then recrystallized from acetone-hexane to yield colorless prisms having a melting point of 74° to 75° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723479 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-8d8d9084812145079c62beccf28cf5f0 |
| 출처 메모 | uspto-grants-1998_03 |