돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1061생성일: 2026년 10월 24일

(E)-ethyl 3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]acrylate → (E)-3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]-2-propen-1-ol

https://huagongshe.com/ko/reaction/1061

반응식

참여 물질

역할이름HCID투입량
반응물(E)-ethyl 3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]acrylateHCID 19694369—
반응물DiisobutylaluminumhydrideHCID 21225700—
생성물(E)-3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]-2-propen-1-olHCID 1969437190%

반응 단계

In the same manner as in Reference Example 11, (E)-ethyl 3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]acrylate was reduced with diisobutylaluminum hydride to yield (E)-3-[5-(5-methyl-2-phenyl-4-oxazolylmethoxy)-2-benzofuranyl]-2-propen-1-ol (yield 90%), which was then recrystallized from ethyl acetate-hexane to yield colorless prisms having a melting point of 145° to 146° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05723479
출처 데이터셋uspto-grants-1998_03
ORD IDord-95e24e77c6ef45318b9ed18596119d65
출처 메모uspto-grants-1998_03