Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Bromo-2,4-dimethoxybenzaldehyde → 5-(3,5-Dimethyl-isoxazol-4-yl)2,4-dimethoxy-benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Bromo-2,4-dimethoxybenzaldehyde | HCID 668346 | — |
| 반응물 | 3,5-Dimethylisoxazole-4-boronic acid | HCID 2734346 | — |
| 생성물 | 5-(3,5-Dimethyl-isoxazol-4-yl)2,4-dimethoxy-benzaldehyde | HCID 21980966 | 75% |
반응 단계
Ex-33A: 5-(3,5-Dimethyl-isoxazol-4-yl)-2,4-dimethoxy-benzaldehyde was prepared from 5-bromo-2,4-dimethoxybenzaldehyde and 3,5-dimethyl-isoxazole-4-boronic acid in a similar manner as described in Ex-3A, 75% yield. 1H-NMR (CDCl3) δ 10.34 (s, 1H), 7.63 (s, 1H), 6.52 (s, 1H), 4.00 (s, 3H), 3.90 (s, 3H), 2.12 (s, 6H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094801B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-cae727d29c5142bab06a1ae4493a7906 |
| 출처 메모 | uspto-grants-2006_08 |