Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Acetate → HCID 2910222, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 반응물 | 4-[(2-Chloro-6-fluorophenyl)methoxy]benzaldehyde | HCID 735467 | — |
| 반응물 | Rhodanine | HCID 1201546 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 2910222 | HCID 2910222 | — |
반응 단계
Under a nitrogen atmosphere in a round bottom flask 4-[(2-chloro-6-fluorophenyl)methoxy]benzaldehyde (1.00 g, 3.78 mmol) was dissolved in acetic acid (19 ml). To this solution was added sodium acetate (1.08 g, 13.2 mmol) and then rhodanine (0.50 g, 3.75 mmol). The reaction mixture was then heated to reflux and maintained at this temeprature. The progress of the reaction was monitored by thin layer chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06251928B1 |
| 출처 데이터셋 | uspto-grants-2001_06 |
| ORD ID | ord-ff225fa8a1734b3aa2a98ab3e16d0410 |
| 출처 메모 | uspto-grants-2001_06 |