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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077521생성일: 2026년 10월 23일

3-(3-Bromophenyl)acrylic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3-bromophenyl)ethenyl)-1,3-diethyl-, (E)-

https://huagongshe.com/ko/reaction/1077521

반응식

참여 물질

역할이름HCID투입량
반응물3-(3-Bromophenyl)acrylic acidHCID 36251—
반응물5,6-Diamino-1,3-diethyluracilHCID 4572133—
생성물1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3-bromophenyl)ethenyl)-1,3-diethyl-, (E)-HCID 644893051.1%

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.52 g (11.1 mmol) of 3-bromocinnamic acid. Then, the resultant crude crystals were recrystallized from tetrahydrofuran/water to give 2.01 g (yield 37%) of Compound 161 as pale green plates.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-8fa31f38f45f41dbbfc33d97a4a47794
출처 메모uspto-grants-1996_08