Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Diethyl 3-(4-chlorophenyl)-2-isoxazolin-5-ylmethylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Chlorosuccinimide | HCID 31398 | — |
| 반응물 | 4-Chloro-benzaldehyde oxime | HCID 219158 | — |
| 반응물 | Diethyl allylphosphonate | HCID 573014 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Diethyl 3-(4-chlorophenyl)-2-isoxazolin-5-ylmethylphosphonate | HCID 20062407 | 104.5% |
반응 단계
Preparation is carried out as in Example 1 from 23.34 g of 4-chlorobenzaldoxime, 22 g of N-chlorosuccinimide, 29.5 g of diethyl allylphosphonate and 22.9 ml of triethylamine in dichloromethane and provides 52 g of oily product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-abc093e2107b434cbc94fb24708993c0 |
| 출처 메모 | uspto-grants-1991_04 |