Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Naphthalenedicarboxylic anhydride → Methyl 3-(1,3-dioxo-1,3-dihydro-benzo[e]isoindol-2-yl)-2-(2-methyl-[1,3]-dioxolan-2-yl)propionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Naphthalenedicarboxylic anhydride | HCID 21437 | — |
| 반응물 | Methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982209 | — |
| 생성물 | Methyl 3-(1,3-dioxo-1,3-dihydro-benzo[e]isoindol-2-yl)-2-(2-methyl-[1,3]-dioxolan-2-yl)propionate | HCID 21982268 | — |
반응 단계
Methyl 3-(1,3-dioxo-1,3-dihydro-benzo[e]isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.45 g, 58%) in the same manner as described in the above example 5 (1) from methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.40 g, 2.11 mmol) and 1,2-naphthalic anhydride (0.55 g, 2.75 mmol), and the obtained product was identified with the following NMR data.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094908B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-507b77cf8a6148b682e37f9d01ce208c |
| 출처 메모 | uspto-grants-2006_08 |