Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylpropylenediamine → 4,4-Dimethyl-2-undecyl-2-imidazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylpropylenediamine | HCID 13128 | — |
| 반응물 | Dodecanenitrile | HCID 17092 | — |
| 용매 | Carbon Disulfide | HCID 6348 | — |
| 생성물 | 4,4-Dimethyl-2-undecyl-2-imidazoline | HCID 178442809 | 78% |
반응 단계
18.31 g (100 mmoles) of undecyl cyanide, 11 g (125 mmoles) of 1,2-diamino-2-methylpropane and 0.5 ml of carbon disulfide were heated at 125° C. for 24 hrs. and then worked up as under Example 23. Distillation at reduced pressure gave 19.66 g (78%) of the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05030629 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-5033a1029d18466ba36806c9e6bafe4f |
| 출처 메모 | uspto-grants-1991_07 |