참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Butyl(dimethyl)silane | HCID 2757279 | — |
| 반응물 | Oxirane, [(10-undecenyloxy)methyl]- | HCID 10353667 | — |
| 생성물 | 11-(Butyldimethylsilyl)undecyl glycidyl ether | HCID 19694625 | 82.6% |
반응 단계
A 100-ml flask equipped with a stirrer was charged with 13.6 g (60 mmol) of 10-undecenyl glycidyl ether, 5.8 g (50 mmol) of butyldimethylsilane and 4 mg (0.01 mmol) of H2PtCl6. The contents were stirred at 60° C. for 24 hours. The resultant reaction mixture was distilled under reduced pressure (145°-154° C./6×10-3 Torr), thereby obtaining 14.15 g (yield: 82.6%) of 11-(butyldimethylsilyl)undecyl glycidyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723497 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-3d817c6e53494262853c2c135e11aa2f |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
