Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexamethylenediamine → N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexamethylenediamine | HCID 16402 | — |
| 반응물 | 1,2-Epoxytetradecane | HCID 18604 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] | HCID 21332395 | — |
반응 단계
In a manner similar to that of Example 1, condensation of 1-tetradecene oxide (91.8 g.) and hexamethylenediamine (25 g.) and recrystallization of the resulting product (71 g., m.p. 118°-121° C.) from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] (I: R = CH3 (CH2)11, R' = H, X = (CH2)6, Z = H) (55.3 g., m.p. 122°-126° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04119668 |
| 출처 데이터셋 | uspto-grants-1978_10 |
| ORD ID | ord-d984b79a673644ef93ab7c2fe01e94be |
| 출처 메모 | uspto-grants-1978_10 |