Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Methoxy-1H-indole-2-carbaldehyde → D-64131
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Methoxy-1H-indole-2-carbaldehyde | HCID 826456 | — |
| 반응물 | HCID 178418255 | HCID 178418255 | — |
| 생성물 | D-64131 | HCID 3921152 | 91% |
반응 단계
Reaction of 5-methoxy-1H-indole-2-carbaldehyde with phenylmagnesium bromide using the procedure described in example 404 gave (805) (91%), mp 159–161° C. 1H NMR δ [(CD3)2SO] 11.86 (s, 1H), 7.94–7.91 (m, 2H), 7.71–7.66 (m, 1H), 7.61–7.57 (m, 2H), 7.42 (d, J=8.9 Hz, 1H), 7.16 (d, J=2.4 Hz, 1H), 7.03 (s, 1H), 6.99 (dd, J=8.9, 2.4 Hz, 1H), 3.77 (s, 3H). Found: C, 76.28; H, 5.21; N, 5.42. C16H13NO2 requires: C, 76.48; H, 5.21; N, 5.57.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094798B1 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-9bcf57638ec4461986b37612b541e68c |
| 출처 메모 | uspto-grants-2006_08 |