Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid → methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid | HCID 19694676 | — |
| 반응물 | methyl N-propyl-4-iodo-2-pyrrolecarboxylate | HCID 19694682 | — |
| 생성물 | methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate | HCID 19694683 | 22.3% |
반응 단계
Following the basic procedure of Example 7(f), by reacting 1.7 g (6 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid with 1.47 g (5 mmol) of methyl N-propyl-4-iodo-2-pyrrolecarboxylate, 450 mg (22%) of methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723499 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-00a204d0f65b435cab8a71dca632e9c7 |
| 출처 메모 | uspto-grants-1998_03 |