Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Phenethylamine → 1-Phenethylamine, (+)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Phenethylamine | HCID 7408 | — |
| 반응물 | (R)-(-)-2-propyloctanoic acid | HCID 208925 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-Phenethylamine, (+)- | HCID 643189 | 88.2% |
반응 단계
Using the crystal comprising (2R)-2-propyloctanoic acid and R)-(+)-1-phenylethylamine (6.8 g) produced in the second recrystallization and acetonitrile (102 mL), the same operation as in the second recrystallization was made to give the crystal comprising (2R)-2-propyloctanoic acid and (R)-(+)-1-phenylethylamine (6.0 g, 98.9% e.e.; yield 88%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07820715B2 |
| 출처 데이터셋 | uspto-grants-2010_10 |
| ORD ID | ord-54191d2ebb5b469a828f5070eff5df6b |
| 출처 메모 | uspto-grants-2010_10 |