Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalic Acid → Ethyltriphenylphosphonium oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalic Acid | HCID 971 | — |
| 반응물 | Oxalic acid dihydrate | HCID 61373 | — |
| 반응물 | Ethyltriphenylphosphonium acetate | HCID 94470 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Ethyltriphenylphosphonium oxalate | HCID 20037189 | — |
반응 단계
To a 2 gallon bottle was charged 1000 g (1.707 mol) of a 70% methanol solution of ethyltriphenylphosphonium acetate.acetic acid complex followed by the addition of 204.4 g (1.622 mol) of oxalic acid dihydrate. The mixture was mixed until all the oxalic acid had dissolved and then about 31.5 g of methanol was added to give a resultant solution of about 50 wt. % ethyltriphenylphosphonium oxalate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04370465 |
| 출처 데이터셋 | uspto-grants-1983_01 |
| ORD ID | ord-6f5673f3b3b14a148c291e99f53885f7 |
| 출처 메모 | uspto-grants-1983_01 |