Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrophenyl chloroformate → 4-Nitrophenyl 2-(3-thiophenyl)ethyl carbonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| 반응물 | Thiophene-3-ethanol | HCID 83731 | — |
| 생성물 | 4-Nitrophenyl 2-(3-thiophenyl)ethyl carbonate | HCID 57094331 | — |
반응 단계
Using the method of Example 7a, 3-thiopheneethanol was treated with 4-nitrophenyl chloroformate to afford, after purification by flash chromatography (EtOAc:hexane (1:9)), the title product (56%); TLC, Rf =0.25, EtOAc:hexane (1:9).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04910190 |
| 출처 데이터셋 | uspto-grants-1990_03 |
| ORD ID | ord-3d3a2ee19fdf416ca2ff9407f0a95d1a |
| 출처 메모 | uspto-grants-1990_03 |