3-Methoxysalicyl alcohol → [3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

HRID 1176466

반응식

HRID 1176466 반응식
[OH:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([O:9][CH3:10])[C:4]=1[OH:11].ClC[CH2:14][CH2:15][O:16][CH3:17]>>[CH3:10][O:9][C:5]1[C:4]([O:11][CH2:14][CH2:15][O:16][CH3:17])=[C:3]([CH2:2][OH:1])[CH:8]=[CH:7][CH:6]=1

참가 물질

3

반응물 2

HCID 780883-Methoxysalicyl alcoholHCID 1189271-Chloro-3-methoxypropane

생성물 1

HCID 43471496[3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

실험 절차

Analogously to Method F, 2.67 g of 2-hydroxymethyl-6-methoxyphenol and 2.19 g of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a colourless oil. Rf=0.23 (1:1 EtOAc-heptane); Rt=3.08.

출처 및 근거

ORD 기록
ord-0e1389e3b17549d1ac151a08daaf8ec4
출처 데이터셋
uspto-grants-2010_11
특허 번호
US07842688B2

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