Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → HCID 178419949, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 4-Morpholinoacetophenone | HCID 38362 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178419949 | HCID 178419949 | — |
반응 단계
A mixture of 2.05 g of 4-morpholinoacetophenone (10 mmol) and N,N-dimethylformamide dimethyl acetal was heated under reflux for 7 hours. The mixture was then mixed with 30 ml of methanol and, after addition of 0.57 ml of hydrazine hydrate, again heated under reflux for about 6 hours. The solid formed on cooling the mixture was filtered off with suction and thoroughly washed with methanol, resulting in 3.8 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728012B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-05e877e49f6e4a7498b3988be9eb552d |
| 출처 메모 | uspto-grants-2010_06 |