Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl isocyanate → 1-Allyl-3-butyl-3-(4-methyl-2-oxazolyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl isocyanate | HCID 15123 | — |
| 반응물 | 2-Oxazolamine, N-butyl-4-methyl- | HCID 12295226 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Allyl-3-butyl-3-(4-methyl-2-oxazolyl)urea | HCID 23468970 | — |
반응 단계
A solution of 2-butylamino-4-methyloxazole (12.0 g, 0.078 mol) and allyl isocyanate (6.46 g, 0.078 mol) in dry benzene was heated under reflux for 4 hours, and worked up as described in Example 3. The product was further purified by chromatography on a silica-gel column, eluting with a 1:1 mixture of benzene and ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04259343 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-a818f0b90bf44e699db9a3fff5848ae3 |
| 출처 메모 | uspto-grants-1981_03 |