Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → titanium(III) trichloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | Diisopentyl ether | HCID 10989 | — |
| 반응물 | titanium(III) trichloride | HCID 10313229 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | titanium(III) trichloride | HCID 10313229 | — |
| 생성물 | I2 di-isoamyl ether | HCID 131712143 | — |
반응 단계
Titanium trichloride composition (A) of 11.0 g was suspended in 55 ml of toluene and iodine and di-isoamyl ether were added in amounts to give a molar ratio of titanium trichloride composition (A)/I2 /di-isoamyl ether of 1.0/0.1/1.0 and then reacted at 80° C. for one hour to obtain titanium trichloride solid catalyst. This catalyst is referred to as titanium trichloride solid catalyst (II).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04259461 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-54247050930040fab4b17de526a68ef3 |
| 출처 메모 | uspto-grants-1981_03 |