Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Molybdenum 2,2,4-trimethyl decahydroquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Azanium bis(dioxido(dioxo)molybdenum) | HCID 21895884 | — |
| 반응물 | 2,2,4-Trimethyldecahydroquinoline | HCID 22628786 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Molybdenum 2,2,4-trimethyl decahydroquinoline | HCID 131710931 | — |
반응 단계
2,2,4-Trimethyl decahydroquinoline molybdate having a 2/1 molybdenum/2,2,4-trimethyl decahydroquinoline molar ratio was prepared as follows. 10 grams 2,2,4-trimethyl decahydroquinoline, 16.30 grams of a 37 wt.% aqueous HCl solution and 250 ml water were dissolved together and heated to reflux in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 28.12 grams ammonium dimolybdate was dissolved in 50 ml hot water. The second solution was added to the first solution. A yellow precipitate formed immediately.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04259491 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-60ebefb24ff74d1690c3e9d29862484a |
| 출처 메모 | uspto-grants-1981_03 |