Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → Allyl 2-fluoro-4-hydroxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | 2-Fluoro-4-hydroxybenzoic Acid | HCID 2783398 | — |
| 생성물 | Allyl 2-fluoro-4-hydroxybenzoate | HCID 14852522 | 69% |
반응 단계
In a manner analogous to Example 1(a), starting with 8.3 g (53 mmoles) of 2-fluoro-4-hydroxybenzoic acid treated for 2 hours at 100° C. with 60 ml of allyl alcohol and 1.5 ml of concentrated sulfuric acid, 7.2 g (69% yield) of the expected ester having a melting point of 80°-81° C. are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05468897 |
| 출처 데이터셋 | uspto-grants-1995_11 |
| ORD ID | ord-03abb826f4a64626b71d362af898e2c2 |
| 출처 메모 | uspto-grants-1995_11 |