참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 4-Formylbenzoic acid | HCID 12088 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 4-Formylbenzoyl chloride | HCID 12424620 | — |
반응 단계
A solution of 4-carboxybenzaldehyde (30.0 g, 0.200 mol) in toluene (300 mL) was treated with thionyl chloride (28.6 g, 0.240 mol) and DMF (1.0 mL). The reaction mixture was heated at 100° C. for 2 h, during which time the solids dissolved to yield a pale yellow colored solution. The reaction mixture was cooled to 0° C. to yield a solution of the title compound in toluene, which was used without further manipulation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07728129B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-abc6f75142d542af8371fa9c0841d003 |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
