Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Ethyl Ketone → Ethanol heptane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Ethyl Ketone | HCID 6569 | — |
| 반응물 | Hydralazine Hydrochloride | HCID 9351 | — |
| 용매 | Methanol--water (1/1) | HCID 22242641 | — |
| 생성물 | Ethanol heptane | HCID 22502148 | 78% |
반응 단계
A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728133B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-38722a7553584aeca29efcd3a8985b6f |
| 출처 메모 | uspto-grants-2010_06 |